GCMS analysis results for sample AD29522, Jan 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC3101\29522.D Vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************** *.* ********************* Peak Number 19 Spiro[3-cyclohexene-1,2'-[2H]f Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

38.40 66.73 ug/1 25489300 Perylene-dl2 37.12

Hit#, of 3 Tentative ID MW MolForm CAS# Qual

1 Spiro [3-cyclohexene- 1,2 1 - [2H] furo [3 406 C26H30O4 031642-63-4 9 2 1H-Dicyclooct[e,g] isoindole-1,3 (2H) 391 C26H33NO2 051624-51-2 3 3 5H-Pyrano [3,2-d] oxazole-6,7-diol, 5 391 C19H21NO8 010380-87-7 1

Abundance Scan 3633 (38.400 min): 29522.D (-) m/z 105.05 100.00% 1(15

391 5000 -

• m/z-> 0- —

Abundance 51

50 I11251451144 100I 150 200 -- 191 215235 269 250 1 300 301 I 1327 350 #54424: Spiro[3-cyclohexene-1,2'-[2H]furo[3,2-f][1 Jbenzopyr 360 400 410 447 450 38.00 38.20 38.40 38.60 38.80 m/ z 391.20 62.27%

391

TT-p-r-r-r-j-r-r 5000 189 38.00 38.20 38.40 38.60 38.80 m/ Z 38.59% — 267 I m/z-> 50 100 150 200 250 300 350 400 450 Abundance #53187: 1H-Dicvclooct[e,g]isoindole-1.3(2H)-dione, 3a,3b.4. 391 । I ' ' ' ' I 1 ' 1 ' I --..... 38.00 38.20 38.40 38.60 38.80 5000 m/ z 00 22.05%

92 175 217 245 .! i l 322 364 1 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #53162: 5H-Pyrano[3,2-d]oxazole-6,7-diol, 5-[(acetyloxy)met I 105 38.00 38.20 38.40 38.60 38.80 I m/ Z 19.32% 5000 146

m/z-> I 50 100 X 150 200 250 300 331 LL 350 391

400 450 ।-i-i—i—i—। i । । । । । ft 1 I 1 ■ • ■ i ' ■ 38.00 38.20 38.40 38.60 38.80

29522.D GCMS1126.M Fri Jan 18 16:49:35 2002 Page 19

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