Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.
NYC-WTC_000036752–000036778Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC3101\29522.D Vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 Spiro[3-cyclohexene-1,2'-[2H]f Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
38.22 71.93 ug/1 27472600 Perylene-dl2 37.12
Hit# of 3 Tentative ID MW MolForm CAS# Qual
1 Spiro[3-cyclohexene- 1,2[2H]furo[3 406 C26H30O4 031642-63-4 9 2 1H-Dicyclooct [e,g] isoindole-1,3 (2H) 391 C26H33NO2 051624-51-2 3 3 5H-Pyrano [3, 2-d] oxazole-6,7-diol, 5 391 C19H21NO8 010380-87-7 1
Abundance Scan 3613 (38.217 min): 29522.D (-) m/z 105.05 100.00% 1(15 i 391 5000
m/z-> 0- —
Abundance 51
50 1 100l 1128,1165,191 215225 269 311327 ,360. 150 200 250 TT 300 T TT 350 |
#54424: Spiro[3-cyclohexene-1,2’-[2H]furo[3,2-f][1]benzopyr | 400 r i 410 447 450 37.80 m/z 3 91 38.00 38.20 38.40 63.43% • I • ' 38.60
301
5000 189 37.80 38.00 38.20 38.40 38.60 m/z 406.20 38.84% I , —..... 7 miz—> 50 100 150 200 250 300 350 400 450 Abundance #53187: 1H-Dicyclooct[e,g)isoindole-1.3(2H)-dione. 3a.3b.4, 391
37.80 38.00 38.20 38.40 38.60 5000 m/z 91.00 21.87%
92. 175 217 245 322 364 P 1 s .1 1
m/z-> 50 100 150 200 250 300 350 400 450 Abundance #53162: 5H-Pyrano[3,2-d]oxazole-6,7-diol, 5-[(acetyloxy)met i ■ ■ ' ■ i 105 37.80 38.00 38.20 38.40 38.60 m/z 392.20 19.74% 5000- 146
miz-> I 50 100 1150 200 250 300 331
350 391 4, 400 .—450 37.80 38.00 38.20 38.40 38.60
29522.D GCMS1126.M Fri Jan 18 16:49:30 2002 Page 18
NYC-WTC_000036775
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017405
Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder