Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
NYC-WTC_000086788–000086807Folder label: “508 Scan 9/15/01 9/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C;\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample 9/15 Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params; LSCINT.P
Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 39.77 0.41 ug/1 64170 Perylene-dl2 37.28 Hit# of /5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 28 2 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 23 3 1/2-Benzenedicarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 12 4 y-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 12 ^bui^ance Scan 3783 (39.768 min): LBC.D (-) Wz 73 /00 100.00% 7|3
147
5000 221
281' 355 429
•n/z-> 40
50 105 Il U I
100 150 200 r-r-X- 250 J :300 350 400 r, 450 39.40 39.60 39.80 40.00 m/z 147.00 68775% Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73
207 5000 147 39 40 39.60 39.80 40.00____ 34 103 m/z 221.00 45.32% 281 ■. I ■ , T.. 482 50 100 150 200 250 300 350 400 450 Abundance #30949: Mercaptoacetic acid, bis(trimethylsilyl)- 73 147 39 40 39.60 39.80 40.00 5000 m/z 207.00 18.48% 221 45 104 193 I 1 1 ■n/z-> 50 100 150 200 250 300 350 400 450 ^bundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e T 1|7 39.40 39.60 39.80 40.00 m/z 281.05 17.69% 73 5000
45 295 I . I ■n/z-> 50 100 150 200 250 300 350 400 4M ' 39.40 39.60 39.80 40.00
LBC.D NP091101.M Tue Oct 0212:17:50 2001 Page 12
NYC-WTC_000086805
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NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 15 and 26, 2001.
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Standard operating procedure for liquid-liquid extraction specifying drip rates and reagent lot numbers.
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Laboratory results for sample AD22491 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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Laboratory results for sample AD22492 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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Laboratory results for sample AD22493 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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