Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
NYC-WTC_000086788–000086807Folder label: “508 Scan 9/15/01 9/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On : 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample : 9/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
41.77 0.43 ug/1 67814 Perylene-dl2 37.28
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4/5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 17 2 Benzophenon^2,4 ', 5-tricarboxylic a 356 C19H16O7 . 000000-00-0 10 3 9H-Purin-6-/mine, N-methyl-9-(trime 221 C9H15N5Si 032865-83-1 9 4 Oxazole, 2 /s-diphenyl- 221 C15H11NO 000092-71-7 9 Abundance Scan 4001 (41.769 min); LBC.D (-) 221
5000 355 281 429 96 T 45 I ^^5 327
Ti/2-> I''' 'I 4 I 253 40 60 80 1 00120140160180 200220240260280300 320340360380400 420 __£L40__4t60_4t80__4Z0g___ m/z 147.00 93^73% Abundance #41682; 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4.4,5,5,7,7- 147 2!1
73 ............................ 5000 41 40 41.60 41.80 42.00 191 m/z 221.00 82.92% 117 279 I I 40 60 80 100120140160180200 220240260280300320340360380400420 ^bundance #49884: Ben2ophenone-2,4',5-tricarboxylic acid, trimethyl e 211 163 41 40 41.60 41.80 42.00 552 m/z 207.00 65791% 356 325 76 103 135 i""i I" " I tVz-> 40 60 80 100120140160180200220240 260 280300320340360380400420 Abundance #27775; 9H-Purin-6-amine, N-methyl-9-(trimethylsilyl)- 2il 41.40 41.60 41.80 42.00 m/z 355.0038.84% 73 5000
Ti/z-> 45
T 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 41.40 41.60 41.80 42.00
LBC.D NP091101.M Tue Oct 02 12:17:54 2001 Page 13
NYC-WTC_000086806
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NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086981
Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069154
Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Standard operating procedure for liquid-liquid extraction specifying drip rates and reagent lot numbers.
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Laboratory results for sample AD22491 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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Laboratory results for sample AD22492 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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Laboratory results for sample AD22493 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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