NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3
Acq On 1 Oct 2001 3:40 pm Operator: 209 GALOS
Sample 9/15 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 13 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T,
41.77 0.43 ug/1 67814 Perylene-dl2 37.28
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4/5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 17
2 Benzophenon^2,4', 5-tricarboxylic a 356 C19H16O7 000000-00-0 10
3 9H-Purin-6-/mine, N-methyl-9-(trime 221 C9H15N5Si 032865-83-1 9
4 Oxazole, 2/5-diphenyl- 221 C15H11NO 000092-71-7 9
^bundance Scan 4001 (41.769 min); LBC.D (-) m/z 73.00 100.00%
73
221
5000 355
281
429
96
TlZz->
45
253,,
40 60 80 100120140160180200220240260280300320340360380400420
1
I
327 .
I I 1 41 40 41.60 41.80 42.00
m/z 147.00 93773%
Abundance #41682:3,6-Dioxa-2.4.5,7-telrasilaoctane, 2,2,4.4.5.5,7,7-
147 z;i
73
5000
41.40 41.60 41.80 42.00
191 m/z 221.0082.92%
117 279
I , r"'i
n/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #49884: Benzophenone-2,4',5-tricarboxylic acid, trimethyl e
2il
163 I ' ' ' ' I ' ' ' ' I ‘ ‘ ' I '
41 40 41.60 41.80 42.00
5000 m/z 207.00 6^791%
356
325
76 103 135
7TTTT7rTT(7rTTT|VTTI7rTTV]-rt-^^
Tife-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #27775: 9H-Purin-6-amine, N-methyl-9-(trimethylsilyl)-
2i 1 41,40 41.60 41.80 42.00
m/z 355.0038.84%
73
5000
45
p-r , 11, 11 I . . . 11,1 I, I
165 192
rrlrrVM^
..... /.J, A
r " 'I''" I
Ti^-> 40 60 80 100120140160180200220240260280300320340360380400420 41.40 41.60 41.80 42.00
LBC.D NP091101.M Tue Oct 02 12:17:54 2001 Page 13
NYC-WTC_000086642
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