GC/MS calibration report for TCLP method, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 3-Isopropoxy-l,1,1,7,7,7-hexam. Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

41.70 0.85 ug/1 83064 PerYlene-dl2 37.23

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-aZl/1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 33 2 1,2-Benzenedi^arboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 17 3 Trisiloxar^ 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 12 4 3,6-Dioxi 2,4,5,7-tetrasilaoctane. 294 C10H3002Si4 004342-25-0 12 Abundance X Scan 3994 (41.705 min): LB.D (-) m/z 73700 100.00%! 70 147

221 5000- 281 355 "ri'". > I > > > ■ ■ 1 > '“'“I

41 429 41.40 41.60 41.80 42.00 V'' I ........I. m/z 147.00 ^“8374^ ■nZz-> 50 W 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ................. HI 147 41.40 41.60 41.80 42.00 m/z 221.05 67737% 221 281 327 .. ).. ,1 , , ... 5^... 50 100 150 200 250 300 350 400 450 500 550 Abundance #72972: J ,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e. 147 ................. 73 41.40 41.60 41.80 42.00 5000- m/z 354.95 28.61%

295 119 , ■ I'' M''' , I.,. J... I.... I.., .7,.......... TiZz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet T* J T 41.40-41.60^ 41.80 42.00 1'

m/z 207.00 27.70% 281 5000

369 I...... ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 41.40 41.60 41.80 42.00

LB.D NP091101.M Thu Oct 18 10:44:09 2001 Page 15

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