Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
I Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 2 09 G7VLOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ***************************************************************** *■* * * * * *
Peak Number 16 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 44.17 0.51 ug/1 50211 Perylene-dl2 37.23 Hit# Of 5 T^tative ID MW MolForm CAS# Qual 1 3,6-Dioxa;X, 4,5,7-tetrasilaoctane, 294 C10H30O2Si4 004342-25-0 38 2 Trisilo; lie, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 27 3 Tris(tX .methylsilyl) borate 278 C9H27BO3Si3 004325-85-3 12 4 TrisjkT oxane, octamethyl- 236 C8H24O2Si3 000107-51-7 10 Abundance '' Scan 4263 (44.174 min): LB.D (-) m/ z 72.95 100.00% 73 147 221
253 281
Tife-> Abundance 43 96 I " *' I 191 I"" I XXUr 40 60 80 100120140160180200220240260280300320340360380400420 Jl #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 2:1 429 I" '' I 43.80 44.00 44.20 44.40 44.60 m/z 147.0090.01%
73 ..... 5000 43.80 44.00 44.20 44.40 44.60 191 m/z 220.9578.57% 117 279 ..... ......... 111.......................... I I..... ................... I.............. Tl/Z-> 40 60 80 100120140160 '180200220240260280300320340360380400420 Abundance #52459: Trisiloxane, 1.1.1,5,5,5-hexamethyl-3,3-bis[(trimet 73 1 17 I ' ' ' ' I ' ' ' ' I’ ' ' 'I ' 281 43 80 44.00 44.20 44.40 44.60 5000 m/z 281.00 44.06%
369 338 Tl/Z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #39028; Tris(trimethylsilyl)borale 73 221 ■ -.43 SO-44.00 44.20 44.40 44.60 m/z^55.05 32.82%
5000 263 133 175 I ‘ * 'I ■n/2-> 40 60 80 100120140160180 200220240260280300 320 340 360380400 420 43.80 44.00 44.20 44.40 44.60
LB.D NP091101.M Thu Oct 18 10:44:11 2001 Page 16
NYC-WTC_000088721
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
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