Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
1’ Library Sear ch _Cprapouncl_Rep.or t__ _
Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator; 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P
Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T.
47.31 0.45 ug/1 44174 Perylene-dl2 37.23
Hit# of 5 Tentative ID MW MolForm CAS# Qua!
1 3,6-Dioxa-2,^, 7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 38■ 2 1-MonoIino'IXoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 25. 3 Trisiloxi fe, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 10 4 Butanoizf acid, 3-methyl-3-[(trimeth 262 CllH26O3Si2 . 055124-90-8 10 Abundance Scan 4605 (47.314 min): LB.D (-) m/z 73700 100.00% 147 221
5000 355 281 ................. 191 47.00 47.20 47.40 47.60 40 ■ t 1 ' m/z 147.00 85777% TlZz-> 50 100 150 200 250 300 350 400 450 Wjundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2.4,4.5.5.7,7- 147 2:1
73 5000 47.00 47.20 47.40 47.60 191 m/z 221.05 71.21%
50 100 117
150 I, 200 250 279
300 350 400 450 ^undi #5887-1 ;-1 -Monolinoleoylglycerol trimethylsilyl ether 73
47-00 47.20 47.40 47.60 207 5000 147 m/z 354.9542.69% 34 103 I 281
■n/z-> Abundance — 50 100 150 JUTu 200 250 300 350 400 #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet ~ 450 -78^
'713 ’ — 147 . - 47.00 . 47.20 47.40 ■■47.60 m/z 207.00 31774% 281 5000
369 I Y 33^ J , .............
Tlfe-> 100 150 200 250 300 350 400 450 47.00 47.20 47.40 47.60
LB.D NP091101.M Thu Oct 18 10:44:13 2001 Page 17
NYC-WTC_000088722
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089311
Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069154
Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
Filed in the same folder
NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
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NYC-WTC_000088753
Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.
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NYC-WTC_000088774
Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.
Filed in the same folder