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GC/MS calibration report for TCLP method, Oct 2001

Machine-extracted title · confidence 90%

Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.

NYC-WTC_000088700–000088724

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 16 Oct 2001 4:11 pm Data File: C:\HPCHEM\1\DATA\OCT1601\LB.D Name: lab blk 9/27 Mise: Method: C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title: 209 625/TCLP calibration table 7/16/01 Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc 3,^JlexaHOTTe 6.37 0.5 ug/1 43637 ISTDOl 11.76 1916650 20.0 2<riiexandne 6.48 0.9 ug/1 87989 ISTDOl 11.76 1916650 20.0 6.73 0.5 ug/1 49054 ISTDOl 11.76 1916650 20.0 1 Di-ehlorobenzene - 11.62 0.5 ug/1 49616 ISTDOl 11.76 1916650 20.0 Cye 1-ep en t anc c arbexy 1 29.50 1.4 ug/1 153162 ISTD05 33.12 2140890 20.0 Heptadecane 29.62 0.8 ug/1 85199 ISTD05 33.12 2140890 20.0 Tricosane 30.71 1.3 ug/1 134616 ISTD05 33.12 2140890 20.0 Butyl tetradecanoate 31.64 1.1 ug/1 123027 ISTD05 33.12 2140890 20.0 Tetracosane 31.74 2.6 ug/1 273561 ISTD05 33.12 2140890 20.0 Heneicosane 32.73 2.6 ug/1 276601 ISTD05 33.12 2140890 20.0 Heneicosane 33.69 3.0 ug/1 321477 ISTD05 33.12 2140890 20.0 Heptacosane 34.61 2.1 ug/1 225166 ISTD05 33.12 2140890 20.0 Tetratetracontane 35.50 2.1 ug/1 201579 ISTD06 37.23 1954620 20.0 Hexatriacontane 36.36 1.2 ug/1 120073 ISTD06 37.23 1954620 20.0 3rJ.sopropuxy 1,1,1, T 41.70 0.8 ug/1 83064 ISTD06 37.23 1954620 20.0 3,6 Dioxa 2,4,5,7-te 44.17 0.5 ug/1 50211 ISTD06 37.23 1954620 20.0 3 ,.£--Dirixa 3,4,5,7 t£ 47.31 0.5 ug/1 44174 ISTD06 37.23 1954620 20.0

LB.D NP091101.M Thu Oct 18 10:44:13 2001

NYC-WTC_000088723

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NYC-WTC_000088723Source: NYC Law Department, mirrored locally

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