Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Hexatriacontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.36 1.23 ug/1 120073 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolFonn CAS# Qual / yHexatriacontane 507 C36H74 000630-06-8 91 '^2 Heneicosane 296 C21H44 000629-94-7 90 3 Heptadecane 240 C17H36 000629-78-7 87 4 Docosane 310 C22H46 000629-97-0 86 Abundance Scan 3412 (36.362 min): LB.D (-) m/z57700 100.00% 57
43 71 5000 85
XuU . I . . . . I . , , . I . , T 99 36.00 36.20 36.40 36.60 ..III 155169182 208 281 '' 11'' f 11''' 111''I' ’‘■'■I T' 1'11 ' I”' ' ' ' I ' ' ' ' I ' ' ’ ’ I ' ■ ' ' I ' m/ Z 71.10 66.17% tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #74636: Hexatriacontane 43 57
71 5000 85 .. 36.00 36.20 36.40 36.60 m/z 43.0.0 63773%
m/z-> J .\ H1.1^5 169 183 197 211 VTYTT-TT*Ymp'TVT-T-YT'TrTVyT-T“TTpnn-TT-p-T-T-Tq-T-T-T-T-yT-Tn-T-^^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance__ #42201 ;.Heneicosane__________________ _ - 57 71 .. 85 36.00 36.20 36.40 36.60 5000 m/z 85.05 49.19% 99 ........ , |( J, , J , ,1^7........... ........ ................. ?58, , 296, mZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane ' 1^^'^ I '■ 57 36.00 36.20 36.40- 36.60 -- m/z 41.05 26.61% 71 5000 85
99 4 40
r-p-n-r-p- n-i* J 141 155169 ' I I ' I 11 I I ■ ■ I'' '' 11' I I I I 210 240 I ' ' ' ' I ' ' ‘ ' I ‘ /wwYyi/ ■n/z-> 40 60 80 100 120 140 16Q 180 200 220 240 260 260 300 36.00 36.20 36.40 36.60
LB.D NP091101.M Thu Oct 18 10:44:06 2001 Page 14
NYC-WTC_000088719
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087132
Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089311
Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069154
Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
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NYC-WTC_000088753
Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.
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NYC-WTC_000088774
Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.
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