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GC/MS calibration data sheet for October 5, 2001

Machine-extracted title · confidence 90%

Laboratory data sheet listing extraction dates and calibration results for deuterated standards.

NYC-WTC_000087980–000087999

Folder label: “GC/MS Scan 9/24/01

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NYC 9/11 Public Portal Document

Library Search Compound Report _____ Data File C:\HPCHEM\1\DATA\OCT0401\LB.D Vial: 9 Acq On 4 Oct 2001 11:22 pm Operator: 209 GALOS Sample 9/24 Inst : GC/MS 209 Mise ■ Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Libraisy : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Hexatriacontane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

35.52 1.90 ug/1 304022 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 2 Heneicosane 3 Octadecane 4 Nonacosane 'Abundance 57 Scan 3320 (35.522 min); LB.D (-) 507 C36H74 296 C21H44 254 C18H38 408 C29H60 m/z 000630-06-8 91 000629-94-7 91 000593-45-3 91 000630-03-5 91 57.00 100.00% s 43 71 85 5000

99 35.20 35.40 35.60 35.80 m/z 71.00 68.75% Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #74636: Hexatriacontane 43 517

71 5000- ,,,,, 85 35.20 35.40 35.60 35.80 m/z 43.00 67.58% 97 ] I I II , 1.1 141 155 W9 183 197 211 ............. in/2-> 4'0 60 80 160 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane — 57 71 85 35.20 35.40 35.60 35.80 5000 m/z 85.05 51.48% 99 I I', : .'1, . I,,,. I..,. I.... I.,. ■ |?9?. I. . !n/z-> 40 60 80 1QQ__12O_J4O_J6O_18O_^^ Abundance #71561: Octadecane 7-^ T 35.20 35.40 35.60 35.80 43 71 m/z 54.9,5 24.87% 85

99 'tJ ."I,. 100 120 140 160 ...... ........... 180 '260 ^0 24o' 2^ 280 300 m/z-> 40 60 80 35.20 35.40 35.60 35.80

LB.D NP091101.M Tue Oct 09 12:53:35 2001 Page 12

NYC-WTC_000087997

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NYC-WTC_000087997Source: NYC Law Department, mirrored locally

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