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GC/MS calibration data sheet for October 5, 2001

Machine-extracted title · confidence 90%

Laboratory data sheet listing extraction dates and calibration results for deuterated standards.

NYC-WTC_000087980–000087999

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000087996
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0401\LB.D Vial: 9 Acq On 4 Oct 2001 11:22 pm Operator: 209 GALOS Sample 9/24 Inst : GC/MS 209 Mise •Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Heneicosane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

34.63 1.92 ug/1 330448 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# ■ Qual

1 Heneicosane 296 C21H44 000629-94-7 9L 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Tetracosane 338 C24H50 000646-31-1 90, 4 Eicosane 282 C20H42 ______ 000112-95-8 87 Abundance Scan 3223 (34.631 min): LB.D (-) m/z 57.0,0 100.00% 5(7

5000 85

v_ -r=T-r-p 34.40 34.60 34.80 35.00 , J ......... .................................. I , m/ z 71.00 70.23% hi/z-> 50___ 100.__ 150__ 200 250__ 300 350___ 400 450 500 Sundance #42201: Heneicosane 57

5000 85 V 34.40 34.60 34.80 35.00 m/z 43.05 66.19% |113 I, IJ ,<i, ) '............... , , , I............................. m/z-> 50 100 150 200 250 . 300 350 400 450 500 Abundance #59136: Hexatriacontane 57 I ___ 34.40 34.60 34.80 35.00 5000 85 m/z 85.0,5 48.90% ;! i ; 239 379 407 435 AV'S 506 m/z-> 50 100 150 200 250 300 350^0 450 500 Abundance #73543: Tetracosane 5(7 34.40 34.60 34.80 35.00 m/z 55.00 23.32% 5000 85

- | . I . , ■ ^^^1 .................................................................................

50 100 150 200 250 300 350 400 450 500 34.40 34.60 34.80 35.00

LB.D NP091101.M Tue Oct 09 12:53:17 2001 Page 11

NYC-WTC_000087996

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NYC-WTC_000087996Source: NYC Law Department, mirrored locally

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