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GC/MS calibration data for TCLP method, Oct 2001

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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.

NYC-WTC_000087496–000087516

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0201\LB.D Vial: 2 Acq On 2 Oct 2001 3:06 pm Operator: 209 GALOS Sample 9/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library. : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Hexatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 36.39 0.67 ug/1 93256 Perylene-dl2 37.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Dotriacontane 451 C32H66 000544-85-4 91 Abundance Scan 3415 (36.388 min): LB.D (-) m/z 57.00 100.00% 5(7

5000 85

36.00 36.20 36.40 36.60 36.80 m/z TITOO 73.93% Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane 57

5000 85 J6;P0_3620_ja40_ja60_36^ m/z 43.05 60.46%

' ' ' I ' ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #49558: Heptadecane, 9-octyl- 57

36 00 36.20 36.40 36.60 36.80 5000 85 m/z 85.00 47.22%

I l 310 352 n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 7 36 00 36.20 36.40 36.60 36.80 m/z 55.00 24.56% 5000

•nfe-> 50 85

100 fri^f\'*?91g7225 150 200 250 300 350 379407 400 450 500 550 590618 600 iL 36.00 36.20 36.40 36.60 36.80

LB.D NP091101.M Wed Oct 03 10:10:13 2001 Page 14

NYC-WTC_000087515

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NYC-WTC_000087515Source: NYC Law Department, mirrored locally

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