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GC/MS calibration data for TCLP method, Oct 2001

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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.

NYC-WTC_000087496–000087516

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0201\LB.D Vial: 2 Acq On 2 Oct 2001 3:06 pm Operator: 209 GALOS Sample 9/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Tetracosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 35.53 1.06 ug/1 147163 Perylene-dl2 37.28 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Tetracosane 338 C24H50 000646-31-1 91, 2 Pentacosane 352 C25H52 000629-99-2 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Hexatriacontane__________________ 507 C36H74 000630-06-8 91> Abundance Scan 3321 (35.525 min): LB.D (-) m/z SYTOO 100.00% 57 71 43 85 5000

Tife-> 4bundance XU 40 60 J, 99 Jl 239253 281 ■fl^-rl’p-rfS-pVT-V-|^--rTVp-lS-T-|-VT-T-iYrT'-rT-rT-rTYr-i-iHy-r-r^-T-p^

80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543: Tetracosane 35.20 35.40 35.60 35.80 m/z 71.00 7^723%

43 57 71

5000 85 .-Tl I-. rT| 35.20 35.40 35.60 35.80 99 m/z 43.05 68.42% I 1 || ■’,1^127 155169183197 294 338 11 . ,. IT1111.... I... 1111 i-'i 11 r I, I 'i..111111 I'''' I' I'''' I'''' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73718; Pentacosane 43 57 J 35.20 35.40 35.60 35.80 71 5000 Wz 85.05 57774% 85

1 t '*^^'127141155169183197211225 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 4bundance #71193: Heptadecane 57 35.20 35.40 35.60 35.80 m/z 4^70 5 2 4.14% 71 5000- 85

99 J 2^141155169 210 240 ' I'''' I ‘ I ’ ' ' ' I ' ' f ' I ' ' ' ' f ' ' ' ' I ' '' ' ' I I' " ' I'' " I'' I • •" I'" ■ I" " I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

LB.D NP091101.M Wed Oct 03 10:10:11 2001 Page 13

NYC-WTC_000087514

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