Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample ■: 9/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Tetracosane Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 30.73 0.67 ug/1 107794 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tetracosane 338 C24H50 000646-31-1 91 2 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91\ 3 Tricosane 324 C23H48 000638-67-5 91 4 Eicosane 282 C20H42 000112-95-8 91 ' Abundance Scan 2798 (30.730 min); LBE.D (-) m/z SYTOO 100.00% 57 71 43
5000 85 . .1 V I 99 30.40 30.60 30.80 31.00 .J..",1,60,1.4.. A■ ...................... m/z7171074.11% n/z-> Abundance " 80 ' 'ioo' '1'20 '140 '1'^' 'iso '2(^' '^0 24o' 2^ 2^' #73543: Tetracosane '320 340 I 43 57 71 / 5000 85 30,40 30.60 30.80 31.00 99 m/z 43.00 66.54% I I, il 155169183197 294 338 ft I.... I r,. 11.,.. 111.. I..11 f 111 'I I.11 pTTp-TTn^pn-TTp-TT-rp -p-rr-rp- n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl-
71 30.40 30.60 30.80 31.00 552 85 m/z 85.05 45.02%
'' I'' ....... ............. . Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73318: Tricosane 4(3 57 y.4O 30.60 30.80 31.00 m/z 41.05 28.33% 71 552 85
183197211225 296 324 ft ^[^1 TqrTT-rryVTTT'jTr-T'rT-rTTTTpTT-TpTTn-p-rTTyTTTTym-rY^ ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00
LBE.D NP091101.M Wed Oct 03 14:41:16 2001 Page 10
NYC-WTC_000087147
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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