GC/MS calibration report for TCLP method, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ***************************************** * * ************************** Peak Number 9 Tetracosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.74 2.56 ug/1 273561 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 Tetracosane 338 C24H50 000646-31-1 91'^ 2 Octadecane 254 C18H38 000593-45-3 91 3 Heptadecane 240 C17H36 000629-78-7 91. 4 Eicosane 282 C20H42 000112-95-8 9T Abundance Scan 2908 (31.735 min); LB.D (-) m/z 56795 100.00% . 57

43 71

5000- 85

mV 31,40 31.60 31.80 32.00 I I ri I |T. . I“j I il . j ,V. I pl I I I I |-r|^. I . . I 1 I I I I Ti I I I I I I I I 1 I u I I I I . I I I I . I I 1 I . I . m/^ 71.05 70.16% TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57

5000 71

85 J T 31.40 31.60 31.80 32.00 m/z 41705 65.28% 155169183197 294 338 I' " '. I' TY’ArV-ryr+T- p-rTVyr+ I'''' I'''' I'''' I tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71560; Octadecane __ 43 57

71 31.40 31.60 31.80 32.00 5000 85 m/z 85.05 k 46.87%

99 254 Ji y-n-n-p-m-p r TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #32063: Heptadecane 77-31.40'31.60 31.80L^tOOa.__ 71 ■m/z 41.05 25731%

5000 85 1 99 j J ^127141 196 240 TlZz-> rJk i ‘' I'''' I'''' I'''' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 T 31.40 31.60 31.80 32.00

LB.D NP091101.M Thu Oct 18 10:43:55 2001 Page 9

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