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GC/MS calibration report for TCLP method, Oct 2001

Machine-extracted title · confidence 90%

Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.

NYC-WTC_000088700–000088724

Folder label: “GC/MS Scan 9/27/01”

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Scanned page image, NYC-WTC_000088715
OCR text

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Heneicosane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 32.73 2.58 ug/1 276601 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Heptacosane 380 C27H56 000593-49-7 91 3 Pentacosane 352 C25H52 000629-99-2 91 4 Nonacosane 408 C29H60 000630-03-5 90 Abundance Scan 3016 (32.727 min): LB.D (-) m/z 57.00 100.00% 5(7

! 5000 85

TiZ;-> Abundance lU 169 196 253 p-fTTpT-I-rpTTTlYTTTTpTTTpTTTp-rTTyrTTTpTTTyrT^^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #42201: Heneicosane 32.40 32.60 32.80 33.00 m/z 71.00 69774%

5(7

85 5000 T 32.40 32.60 32.80 33.00 m/T 43705 67.55% I 113 jUXmXvt I . 111111111. .111.. I. I. I n I I ""I" " I 268 296 I " ' ‘ I' " ' I nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52248£Heptacosane 7

32.40 'szeo" 32.8^ 33'00 5000 85 m/z 85.05 48.39%

196 224 281 - 324 380 i ''' ' I " '' I' ‘ " I'' ' ' I I""I""I""I" "I" n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance ,#73718: Pentacosane ................... / \ ............. , 43 ~ 32.40 ~ 32.60 /32.80„33.00 m/z41.05 25791% 71 5000

, 99

nAj-> XU 127 155 183 JTVrrfTTTVpT^rrpTTTTT^^ 211 p-rTTp-rrrpTTTp-rTTTTTTTpT-TTp-rT^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 32.40 32.60 32.80 33.00

LB.D NP091101.M Thu Oct 18 10:43:57 2001 Page 10

NYC-WTC_6obO88715

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NYC-WTC_000088715Source: NYC Law Department, mirrored locally

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