Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Heneicosane Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T. 32.73 2.58 ug/1 276601 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Heneicosane 296 C21H44 000629-94-7 91 2 Heptacosane 380 C27H56 000593-49-7 91 3 Pentacosane 352 C25H52 000629-99-2 91 4 Nonacosane 408 C29H60 000630-03-5 90 Abundance Scan 3016 (32.727 min): LB.D (-) m/z 57.00 100.00% 5(7
! 5000 85
TiZ;-> Abundance lU 169 196 253 p-fTTpT-I-rpTTTlYTTTTpTTTpTTTp-rTTyrTTTpTTTyrT^^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #42201: Heneicosane 32.40 32.60 32.80 33.00 m/z 71.00 69774%
5(7
85 5000 T 32.40 32.60 32.80 33.00 m/T 43705 67.55% I 113 jUXmXvt I . 111111111. .111.. I. I. I n I I ""I" " I 268 296 I " ' ‘ I' " ' I nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52248£Heptacosane 7
32.40 'szeo" 32.8^ 33'00 5000 85 m/z 85.05 48.39%
196 224 281 - 324 380 i ''' ' I " '' I' ‘ " I'' ' ' I I""I""I""I" "I" n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance ,#73718: Pentacosane ................... / \ ............. , 43 ~ 32.40 ~ 32.60 /32.80„33.00 m/z41.05 25791% 71 5000
, 99
nAj-> XU 127 155 183 JTVrrfTTTVpT^rrpTTTTT^^ 211 p-rTTp-rrrpTTTp-rTTTTTTTpT-TTp-rT^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 32.40 32.60 32.80 33.00
LB.D NP091101.M Thu Oct 18 10:43:57 2001 Page 10
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
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