Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 2 09 GTVLOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *********************************************************************** Peak Number 11 Heneicosane Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T. 33.69 3.00 ug/1 321477 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Heneicosane 296 C21H44 000629-94-7 91. 2 Tricosane 324 C23H48 000638-67-5 91 3 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 4 Nonacosane 40'8 C2 9H60 000630-03-5 91 Abundance 57 Scan 3121 (33.691 min): LB.D (-) m/z SYTOO ToYToo? 43 71
5000 85
X TTfe-> 40 XU 60 99 i ’.iJ 155169183197211 226 Tp5-Ti‘yrT¥T-p-/¥Tn7TTTVp-Ti“TYTTTTYrTTTj-rrTTY-rT-^^ 80 100 120 140 160 180 200 220 240 260 280 300 320 253267281 33.40 33.60 33.80 34.00 m/z 71.10 67.99% Abundance #42201: Heneicosane 57 71 85 5000 ... 33.40 33.60 33.80 34.00 99 mZz 43.05 66.94% -n-p-T I . .-i , I r, . ."i . . T. I , ■, , , I . , , ■, I . . , , I I . , , , , , , , I , , , , I , , , , I , , , , I , , , 1 I , , , , I , , m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 5l7 rT=1p‘TT-T-rY-Zm 71 . 33,40 33,60 33.80 34.00 5000 85 ■m/z 85.05 49.10%
- 183197211225 ' 296 324 r ''' I''' ‘ I'''' I'''' 1'''' I'''' I ''''' I'' ‘ I'' ‘' I''' ‘ I''' ‘ I'''' I'''' I'' ‘ mfe-> Abundance 40 60
43 57 80 100 120 140 160 180 200 220 240 260 280 300 320 #50999: Eicosane, 7-hexyl- .. I j-rTT 33.40,33.60 33.80 34.00 ■ m/z 41.05 24.98% 71 5000 85 r/Xn-T I ZVrp-T-mqQ f rt ■'82197 281 310 . I iT-n‘| I ■ I I I I I r rp < > ■ । I'"' I mZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 33.40 33.60 33.80 34.00
LB.D NP091101.M Thu Oct 18 10:44:00 2001 Page 11
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089311
Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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