Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS, Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P
Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L **************************************************** *,* *************** Peak Number 12 Heptacosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 34.61 2.10 ug/1 225166 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
Hep tacosane 380 C27H56 000593-49-7 91 2 Tetracosane 338 C24H50 000646-31-1 90 3 Heptadecane 240 C17H36 000629-78-7 87 4 Dotriacontane 451 C32H66 000544-85-4 87 Abundance Scan 3221 (34.609 min): LB.D (-) m/z 57.00 100.00%! 5(7
5000 85
4 34.20 34.40 34.60 34.80 35.00 I . T. I . . . I f rr.V| I r. . p , , , I . iTi I I . > I I ■ I ■ I I I " I'''' I'' m/z tITOO 68.45% nZz-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #52248: Heptacosane 1 57
5000 85 a ' I ’ ’ 34,20 34,40 34,60 34,80 35,00 niTz 43700 65733% 169 196 224 281 324 380 TTpTTT-p-rrryTvrYp-rrrpT-rTY^ TTp-rrrp-rrTp-rTTp-rTTp-rTTp-rTTp-rTTp-rTTp-rrTp-TT^TTTtrr Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #73543;-Tetracosane-- - - - 57
I ' ' ' ' I 34.20 34.40 34,60 34.80 35,00 5000 85 m/z 85.05 47.70%
113.- ..
nZz-> XU4 - 155 1^' - I'''' I''''' I "'' I' "' I' " ' I'' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 294 338 yrrnyrTTTpTTrpTTTjnT^^
Abundance#711^ Heptadecane _ 5(7 .34.20 - 34.40 - 34.60 . 34,80 35,00- m/z 41.05 23.47%
5000 85. —
I I I q 11 r I I I I I I [■ I I I I I u 11 I I I I I 11 |-nr|-rri’i pi • I'''' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 34,20 34,40 34,60 34,80 35,00
LB.D .NP091101.M Thu Oct 18 10:44:02 2001 Page 12
NYC-WTC_000088717
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
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NYC-WTC_000088753
Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.
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NYC-WTC_000088774
Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.
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