Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Tetratetracontane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 35.50 2.06 ug/1 201579 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Tetratetracontane 619 C44H90 007098-22-8 91s. 2 Heneicosane ■ 296 C21H44 000629-94-7 91 ) 3 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 / 4 Hexatriacontane 507 C36H74 00'0630-06-8 91 ' Abundance Scan 3318 (35.499 min): LB.D (-) m/z 57.00 100.00% 57
5000- 85
, ,■ 11 ] r. , . I'n I I I , 35.20 35.40 35.60 35.80 , 1411691^ ^9 m/z 71.00 66.70% Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 57
5000 85 35.20 35.40 35.60 35.80 m/z 43705 65.85% 379407 590618 r-r-r-p- ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance .. __ #42201; Heneicosane------ — -------- 57
35.20 35.40 35.60 35.80 85 5000 m/z 85.05 48.09% A
H-ry, ■n/z-> Abundance 50
43 100 150 200 250 300 350 400 #51002: Heneicosane, J 1_-{1-ethylpropyl)- 450 500 550 600 _ . ik ---35.20 35.40 35.60 -35,80 --.-- m/z 41.05 23.59% 71 5000
99 ,225 295 338 , , , ■n/z-> 50 100 ■ 150 200 250 300 350 400 450 500 550 600 35.20 35.40 35.60 35.80
LB.D NP091101.M Thu Oct 18 10:44:04 2001 Page 13
NYC-WTC_000088718
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
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NYC-WTC_000088753
Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.
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NYC-WTC_000088774
Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.
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