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GC/MS analysis results for sample AD23124, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23124 conducted on October 12, 2001.

NYC-WTC_000088000–000088022

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088019
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NYC 9/11 Public Portal Document

Library 'Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0401\23124.D Vial: 12 Acq On 5 Oct 2001 2:18 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise •Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heneicosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

35.53 1.59 ug/1 295280 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Tetracosane 338 C24H50 000646-31-1 91 4 Tetratetracontane 619 C44H90 007098-22-8 91 *\bundance Scan 3321 (35.526 min); 23124.D {-) m/z 57.00 100.00% £7

85 5000

nri/Z“>_____ II 50 100 150 200 250 ...... ................ 300 350 400 450 500 35.20 35.40 35.60 35.80 m/z 71.00 73.34% Abundance #42201; Heneicosane 57

85 5000 rA 35.20 35.40 35.60 35.80 113 441 m/z 43.05 67.22% I I J 268 296 m/z--> 50 100 150 200 250 300 350 400 450 500 Abundance #59136; Hexatriacontane 57 P ■' ' ' I 35.20 35.40 35.60 35.80 I 5 i ' 85 m/z 85.0.5 51.88% ! ■ •

I?( 239 ....... 379 407 435 , 478. 506 300 350 ' 400 '450 ' ' '560 m/z-> 50 100 150 200 250 ' Tr ' I ' I ' VjT I I 1 I I . I* r i’ Abundance #73543; Tetracosane 5(7 35.20 35.40 35.60 35.80 m/z 55. 24.28% 5000 85

155 183 294 338 m/z-> 50 100 150 200 . 250 300 350 400 450 500 3k20 35'40' osJeo 35'80'

23124.D NP091101.M Tue Oct 09 12:38:42 2001 Page 13

NYC-WTC_000088019

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NYC-WTC_000088019Source: NYC Law Department, mirrored locally

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