GC/MS calibration table, Oct 1 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\LB.D Vial: 8 Acq On : 30 Oct 2001 9:22 pm Operator: 209 GALOS Sample : lab blk 10/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P . I Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Tetracosane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.69 1.36 ug/l 375475 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-X^§^ 2 Heptadecane 240 C17H36 000629-78-7 91. 3 Heneicosane 296 C21H44 000629-94-7 91 4 Eicosane, 7-hexyl-__________________ 366 C26H54 055333-99-8 91 (Abundance Scan 2902 (31.685 min): LB.D (-) Wz 57700 100.00%.

43 57

71 fl 85 5000

, 99 1^1, ,, I......... .... Mr...... 31.40 31.60 31.80 32.00 MU 80 100 120 140 :i60 180 200 220 2^ 2OT 280 300 320 \m0 m/z 71.10 67789% ■n^-> 40 60 Abundance #73543: Tetracosane 43 57 71

5000- 85 V 31.40 31.60 31.80 32.00 99 m/z 43705 67.86% j 1 || 155169183197 294 338 I'' * 'I' ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #32063:.Heptadecane__________________________ 57 71 85 31.40 31.60 31.80 32.00 5000 J m/z 85.05 52.69% 99

L n/z-> -UW 100 120 140 160 180 200 220 240 260 280 300 320 340 40 60 80 Abundance #42201: Heneicosane 57 — ::2_31.40;,- 31.60 -31.80.z32.00^ 71 m/z 41.00 2^747%

5000 85 I 99 268 296 I» m-| T 1. 11,»T3 j I«1111 >'i 11 p-TTTp-TTTp-rrq- ............ I''' ’ I ‘ I''' I ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

LB.D NP103001.M Mon Nov 05 08:57:05 2001 Page 9

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