GC/MS calibration table, Oct 1 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\LB.D Vial: 8 Acq On : 30 Oct 2001 9:22 pm Operator: 209 GALOS Sample : lab blk 10/1 Inst : GC/MS 209 : Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ' Peak Number 10 Heptadecane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 32.68 1.35 ug/1 373159 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Qua! i 1 Heptadecane 240 C17H36 000629-78-7 91x ' 2 Pentacosane 352 C25H52 000629-99-2 91X. ’ 3 Heneicosane 296 C21H44 000629-94-7 91. ) 4 Tetracosane 338 C24H50 000646-31-1 91 Abundance Scan 3010 (32.677 min); LB.D (-) in/z 567^5 100.00% 57

85 5000 4

nfe-> 40 -Xl 60 197 224239 281 I'' " I' " ' I " '' I'''' I' " ' I " '' I'' ‘' I' " ' I " '' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 352 mTz 32.40 32.60 32.80 33.00 71710 76.11% Abundance #32063: Heptadecane 57

85 5000 ...... H ' ‘ i ' ' 32.40 32.60 32.80 33.00 m/z 43.05 69.59%

Ti/z-> Abundance X to 196 2-W 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m-p

#73718: Pentacosane '' I'''' I'''' I'''' I'''' I'''' I'''' I

43 ■'-m' XL 71 32.40 32.60 32.80 33.00 . 5000 m/z 8571)5 55.37%

“ 183- -211" I''' ' I ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance ■#42201 :Heneicosane ............ 7 32.40 -32.60^ 3286133.00 - m/z 41700 28.12% >• 85 5000

11 |ri 111. iT111 > I. I < I ........................... . ....... ..................................... 11.1111 < 1, 1, 111111,.,, 111,.,.., 1, 1111111111 n 111111 TlZZ-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

LB.D NP103001.M Mon Nov 05 08:57:07 2001 Page 10.

NYC-WTC_000089293