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GC/MS analysis results for sample AD23834, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23834 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089476–000089500

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089491
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\l\DATA\0CT3001\23834.D Vial: 19 Acq On : 31 Oct 2001 8 :04 am’ Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Heptadecane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 30.65 0.81 ug/1 115196 Chrysene-dl2 33.05 Hit# of 5 Tentative ID MW MolForm CAS# Qual.

1 Heptadecane 240 C17H36 000629-78-7 9<. 2 Pentacosane 352 C25H52 000629-99-2 91^ 3 Tricosane 324 C23H48 000638-67-5 91/ 4 Nonadecane 268 C19H40 000629-92-5 :90 ' Abundance Scan 2789 (30.645 min); 23834.D (-) m/z57.00 100.00%, 57 43 71

85 5000

.1, I T 155169183197 30.40 30.60 30.80 31.00 'l . ,7 , . , ,T, I I I , I'''' I'''' I'''' I' ‘' I m/z 71.00 74.79% ■n^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71193; Heptadecane 57

71 5000 85 30.40 30.60 30,80 31.00 m/z43.05 72.25% 99 I J ^P^?7141 155169 210 240 '''' I '''' I'' I'''' I''' ‘ I'''' I ' I ' ' r I I I ■ . . I' I . . . I ■ ■ . I I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73718: Pentacosane —43-5,7 T-+ 71 30.40 30.60 30.80 31.00 5000 m/z 85.05 51.86% 85

m/z->40 60 80 100 120'140 160 180 "260 ^0 240 260 280 300 3^ Naundance #73318: Tricosane -43-57- ----- -30.40-30.60^ 30.80 31.00 " m/'^-4T.05 29.54% 71 5000 85

nZz-> LU I 183197211225 '' I''' 11 ‘' I'' ’' I'''' I ■','' T''' ■' I'''' I ■'''' I'''' I'''' I'''' I''' ‘ I''' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 296 324 30.40 30.60 30.80 31.00

23834.D NP103001.M Thu Nov 01 13:21:42 2001 Page 9 .

NYC-WTC_000b89491

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NYC-WTC_000089491Source: NYC Law Department, mirrored locally

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