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GC/MS calibration table, Oct 1 2001

Machine-extracted title · confidence 100%

GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.

NYC-WTC_000089278–000089298

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089291
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT3001\LB.D Vial: 8 Acq On : 30 Oct 2001 9:22 pm Operator: 209 GALOS Sample : lab blk 10/1 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DAT7kBASE\NBS75K.L ********************************************* *■* **********************

Peak Number 8 Butyl tetradecanoate (myristat Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 31.59 0.99 ug/1 272746 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl-tctrndCganoate (myristate) 284 C18H36d2 000000-00-0 58 2 Octadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 53 3 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 45 4 1-Hexene, 2-methyl-98 C7H14 006094-02-6 27 <\bundance Scan 2892 (31.594 min): LB.D (-) m/z 56.00 100.00% 5b

5000 4 129 jjj Jill 11 '*,11 [ ''.^157171 J ^199213227^'*'' J I rii I I I iTp I TT j I fl i j 1 I I I I I I I I j I'l 1 I *1 I I I 1 I r'l J I I I IT 267 285 340 IK 31.20 31.40 31.60 31.80 32.00 in/z 57.00 52.24% TT/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 55

5000 229 jM 31,20 31.40 31.60 31.80 32.00 I 73 129 211 m/z 43.05 39707% 185 284 I '11>.11.... 11... I I'''' I ‘ ‘' T‘ ‘ ‘ 1 ttZz-> 40 60 80 100 120 140.160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester_________________ , 5b

31.20 31.40 31.60 31.80 32.00 5000 m/ z 41.05 32774% 285 340, 73 267 129

n/z-> 40 60 I I '' ' ' I ' ' ' ' I '' ' ' I' ' ' ' I ' ' ' ' p' ' 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I' " ' I

Abundance #48214: Octadecanoic acid, 2-methylpropyl ester ’ ------ 5|7 31.20 -31.40-31.60-31.80 ' 32.00 m/z 55.00 27.94%

5000 285 267 J T ijiii 241 1 I 340 i I I I I . I I p-i I r I I I r. j p ‘ ' I ' ' ‘ I ' ' ' ' I ' ' ' ' 1'^' ' I ’ ' ' ' I p—7-, : i~ ~ I • ri' I ~ ■ ■ r I ■ r I 77*.^ ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 - •31.20 31,40 31.60 31.80 32.00

LB.D NP103001.M Mon Nov 05 08:57:03 2001 Page 8 I

NYC-WTC_000089291

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NYC-WTC_000089291Source: NYC Law Department, mirrored locally

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