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GC/MS analysis results for sample AD22582, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22582.D Vial: 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Heneicosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.77 1.18 ug/1 162025 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Tetratetracontane 619 C44H90 007098-22-8 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Pentacosane 352 C25H52 000629-99-2 91 Abundance Scan 2911 (31.767 min): 22582.D (-) m/z 56795 100.00% 57

5000- 85

' I ' ' ' I 31.40 31.60 31,80 32.00 m/z-> sb' 100' 150 '200 '2^ 300' '460 '5^' 600 m/z71.05 70.10% Abundance #42201: Heneicosane 57

85 5000 31.40 31.60 31.80 32.00 m/z 43700 65.43% J ,.... .................... m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 57

31.40 31.60 31.80 32.00 5000 m/z 85.00 44787% 85

j I^Pi'*^\'»?9l?7225 379^7 590618 TTfe-> Abundance 50

57 100 150 200 250 300 350 400 #71561: Octadecane 450 500 550 600 a/L- r- ' '' I ' ’ ’ ' I 31.40 31.60 31.80 32.00 m/z 41.00 23.26% 85 5000

J IS 2242^-* 50 100 150 200 250 300 350 400 450 500 550 600 31.40 31.60 31.80 32.00

22582.D NP091101.M Wed Oct 03 12:09:14 2001 Page 8

NYC-WTC_000087265

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NYC-WTC_000087265Source: NYC Law Department, mirrored locally

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