Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Se^ch Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\MBS75K.L ********************************************************************* Peak Number 8 Butyl tetradecanoate (myristat Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 31.64 1.15 ug/1 123027 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual
Butyr tetradecanoate (myristate) 284 C18H36O2 000000-00-0 80 2 Octadecanoic acid, butyl ester 340 C22H44O21 000123-95-5 42 3 Cyclohexaneacetic acid, butyl ester 198 C12H22O2 027948-12-5 32 4 1-Pentene, 2,4-dimethyl-____________ 98 C7H14 002213-32-3 27 ' Abundance Scan 2898 (31.643 min): LB.D (-) m/z 56700 100.00% 55
5000 4' 73 I Q7 285 31,40 31.60 31.80 32.00 340 .. 11, .Tf . T.. I r.. 11... r I.... I , I,.., I.,,. I,, 111..,. I.,,, I,;,, I r,,, I,, '' I'''' I'' m7z 57700 53.65% tVz-> Abundance 40
53 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #40186: Butyl tetradecanoate (myristate) A 5000 229 31.40 31.60 31.80 32.00 211 m/z 43705 39.73% .. T,„. ' I'''' I " '' I' TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance _ #73570: Octadecanoic acid, butyl.ester____ ___ sis’
31.40 31.60 31.80 32.00 5000 m/z 41.05 37.68% 285 340 73 267 129
■nfe-> 40 60 4. 80 I ' •' 'I' ' k ' I ' -z±!_Lj 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #22409: Cyclohexaneacetic acid, butyl ester r-iTT-rTT-r-r-rqp-r-rT-p-T-V'r'l-^^ — 55 ____ ^31-.4O. 31.60, 31.80 32.00 - “fn/z 55.00 31.59%
5000
125 81 97 143
■nZz-> 40 60 UUUr 1__________ 198 _ ' I'''' I'''' I ’' " I " '' I'''' I'''' I'''' I'''' I'''' I ■'' ’ I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I 31.40 31.60 31.80 32.00 '
LB.D NP09T101.M Thu Oct 18 10:43:53 2001 Page 8
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089311
Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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