Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
NYC-WTC_000087132–000087155Folder label: “508 Scan 9/18/01 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBE.D Vial: 5 Acq On : 1 Oct 2001 5:38 pm Operator: 209 GALOS Sample : 9/18 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Nonacosane Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 29.66 0.44 ug/1 71795 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Nonacosane 408 C29H60 000630-03-5 91' 2 Dotriacontane 451 C32H66 000544-85-4 91 3 Heneicosane 296 C21H44 000629-94-7 90' 4 Heptadecane 240 C17H36 000629-78-7 87 Abundance Scan 2681 (29.656 min): LBE.D (-) m/z 57700 100.00% 57 J 5000 85
'r 29.40 29.60 29.80 30.00 I ll^P.141 168 m/z 43.05 717776% ■rVi-> 50 100 150 200 250 300 350 400 450 Abundance #54526: Nonacosane 43
5000 71
m/z Ma 29.40 29.60 29.80 30.00 71.00 T
67.98%
■nZz-> Abundance 50 I 99 J H ,11?^,......................................... ??. 100 150 200 250 300 #74490: Dotriacontane 350 400 ......... 450 AA 43 , AAa.. 29.40 29.60 29.80 30.00 71 5000 m/ z 85.05 49.00% fl 97 ' ' I ,'L ..............................yy,, mfe->50 100 150 200 250 300 350 400 450 Abundance #42201: Heneicosane 57 29.40 29.60 29.80 30.00 m/z 41.00 30.09% 5000 85 A I 113 I,, J J , ........ 2^, 296 ......... ■n/z-> 50 100 150 200 250 300 350 400 450 29.40 29.60 29.80 30.00
LBE.D NP091101.M Wed Oct 03 14:41:14 2001 Page 9
NYC-WTC_000087146
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NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 18 and 27, 2001.
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NYC-WTC_000087008
Technical form recording liquid-liquid extraction parameters including drip rates and pH measurements for WTC samples.
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NYC-WTC_000087013
Gas chromatography-mass spectrometry analytical report for sample AD22548 completed on 9/27/01 identifying other unknown compounds.
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NYC-WTC_000087022
Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.
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NYC-WTC_000087044
Laboratory report documenting GC/MS analysis of sample AD22550 conducted on September 27, 2001, identifying unknown compounds.
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