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GC/MS calibration table, Oct 2001

Machine-extracted title · confidence 50%

Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.

NYC-WTC_000086624–000086643

Folder label: “508 Scan

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Scanned page image, NYC-WTC_000086641
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NYC 9/11 Public Portal Document Librai?y Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On : 1 Oct 2001 3:40 pm Operator: 209 GALOJ Sample : 9/15 Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 39.77 0.41 ug/1 64170 Perylene-dl2 37.28 Hit# of /5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 28 2 Mejzcaptoacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 23 3 1/2-Benzenedicarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 12 4 /-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 12 Abundance Scan 3783 (39.768 min): LBC.D (-) 73 147

5000 221

281 355 40 105 39.40 39.60 39.80 40.00 m/z 147.00 68.75% Tl/Z-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 . ... _39xg_ja6g_39,8o_4aog___ 34 103 m/z 221.00 45.32% 281 , I III J ■ 1 , T. 482 n/z-> 50 100 150 200 250 300 350 400 450 Abundance #30949: Mercaptoacetic acid. bis(trimethylsilyl)- 73 147 39 40 39.60 39.80 40.00 5000 m/z 207.00 18.48% 221 45

Tl/Z-> LX 50 100 150 200 ... 250 300 350 400 450 Abundance if72972-. 1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e T 1|7 39 40 39.60 39.80 40.00 m/z 281.05 17.69% 73 5000

TlZz~> 45

' I I 50 100 150 200 221 ,T.,,, 2^' ' 300 ' ' 3M ' ' 400 ' ' 450 39.40 39.60 39.80 40.00

LBC.D NP091101.M Tue Oct 02 12:17:50 2001 Page 12

NYC-WTC_000086641

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NYC-WTC_000086641Source: NYC Law Department, mirrored locally

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