Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
NYC-WTC_000033707–000033722Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV2601\LBA.D Vial: 9 Acq On : 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample : 11/20 lab bik scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K . L *************** ****************************************************** Peak Number 3 1-Monolinoleoylglycerol trimet Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
36.72 0.91 ug/1 176851 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 23 2 1,1,1, ,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 17 3 Tris(t imethylsilyl) borate 278 C9H27BO3Si3 004325-85-3 12 4 1,2-Be nzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 10 Abundance 7 Scan 3451 (36723 min): LBA.D (-) m/z 73.00 100.00% 73 147 5000 221 281 355 . .. 429 36.40 36.60 36.80 37.00 43 TT ,94 119—1 , ' 100 150 1 191 ■— — 11 1 32544 , , 401 4— m/z 147.00 65.56% m/z-> 50 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73
207 5000 147 36.40 36.60 36.80 37.00 34 103 m/z 221.05 48.88% ' 1 I* —. |. —.281—. '. ।. - 395
..JC 482 50 100 150 —— m/z-> 200 250 300 350 400 450 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 ' 1,11"'1 T T"T. ‘ ■ • ’ i ’ • • « i • t > । । 147 36.40 36.60 36.80 37.00 267 m/z 281.00 28.32% 5000 __ 355 429 45 207
mz-> 1—0 50 100 hl,.... —.... 150 200 250 300 350 400 450 Abundance #39028: Tris(trimethylsilyl)borate 73 221 36.40 36,60 36.80 37.00 ' m/z 354.95 21.70% 5000 263 133 175 ...... 50 -- 100 150 4 200 ~ ■ i — 111 i ■ — 1 । IPP ‘T m/z—> 250 300 350 400 450 36.40 36.60 36.80 37.00
LBA.D GCMS1126.M Tue Nov 27 12:44:17 2001 Page 3
NYC-WTC_000033715
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NYC-WTC_000033886
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030685
Header page for a gas chromatography-mass spectrometry scan file related to environmental testing at the World Trade Center site.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047955
GCMS blank analysis report for sample AE08209 listing volatile organic compounds from April 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder
NYC-WTC_000033731
Laboratory report detailing GCMS analysis of sample AD28145 conducted on November 29, 2001, noting unknown compounds.
Filed in the same folder