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GCMS blank analysis results for sample AD28143, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.

NYC-WTC_000033707–000033722

Folder label: “GCMS X 11/20/01 A 11/26/01”

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Scanned page image, NYC-WTC_000033716
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV2 601\LBA.D vial: 9 Acq On 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample 11/20 lab blk scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Propanamide Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 38.00 0.44 ug/1 85848 Perylene-dl2 37.12 Hit# of Tentative ID MW MolForm CAS# Qual 1 Propa:namide 73 C3H7NO 000079-05-0 5 2 Benzeneethanamine, N-methyl - 135 C9H13N 000589-08-2 4 3 Dextroamphetamine 135 C9H13N 000051-64-9 3 4 Carbon dioxide 44 CO2 m/z 000124-38-9 3 39.90 100.00% Abundance” Scan 3590 (37.999 min): LBA.D (-) 40

5000

73 I ' 1 1 1 1 ' ■ TT—nnmm 37.60 37.80 38.00 38.20 38.40 I 103 117 253 281 200221 250 150 191 1300325355 , 429 1350 1400 m/z 43.95 57.37% m/z-> 50 100 Abundance #62531: Propanamide 44

5000 73 37.60 37.80 38.00 38.20 38.40 m/z73.00 13.37% 15 t — tr ' 1 1.. TT.. I.. ’.. 11... TTT r > । TT..T.. TT m/z-> 50 100 150 200 250 300 350 400 Abundance #6311: Benzeneethanamine, N-methyl- 44 T TT 37.60 37.80 38.00 38.20 38.40 5000 m/z 147.00 11.10%

6591 135.......... '....................................... i • 1 * ‘ r1 • 1 ■ i ' * 1 ■ i 1 ' ■ ‘ j 1 1 1 ■ । 1 1 1 1 i 1 ■ 1 1 i 1 m/z-> 50 100 150 200 250 300 350 400 Abundance #65628: Dextroamphetamine 44 37.60 37.80 38.00 38.20 38.40 m/z 220.95 7.68% 5000

- 91

m/z—> — 50 5.120 100 150 ' 50 300 350 400 .... i. —.—।. '. - 37.60 37.80 38.00 38.20 38.40

LBA.D GCMS1126.M Tue NOV 27 12:44:19 2001 Page 4

NYC-WTC_000033716

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NYC-WTC_000033716Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28157, Nov 2001 · Box DEP Box 21

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GCMS comments for sample AD28149, Nov 2001 · Box DEP Box 21

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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

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