GCMS unknown compound analysis, sample AE05518, April 2002

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4 Library Search Compound Report I Data File C:\HPCHEM\1\DATA\APRO102\5518.D Vial: 9 Acq On 1 Apr 2002 8:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Propanamine Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.22 0.63 ug/1 93162 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l-Propanamine 59 C3H9N 000107-10-8 9 2 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 3 Butane / 58 C4H10 000106-97-8 9 4 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 9 iAbundance .......... Siran346l(a^5nin)^^ m/z. o's'.... 100?^ 4)3

59 5000 .... 101 7.80 8.00 8.20 8.40 8.60 83 ' I ' ' ' ' I ' ' ' ' I m/ z 55.22% m/z->10 20 30 40 50 60 70 80 90 100 110 Abundance #62341: 1-Propanamine 30

5000 V 2:80^_.8;0o__a2g_84g__8^^ 59 m/z 100.95 20.33% ....... 37 ......... ,.1......... ..... \........ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1840: Morptioiirie. 4-mettiyl- I 43

7.80 8.00 8.20 8.40 8.60 5000 m/z 13.96% 101 15 71 27 i • II, 56

__ 10 20 30 40 50 _60 70 80 90 100 110 p>ibundance #6f336: Butane 40 7.80 8.00 8.20 8.40 8.60 m/ z 41,.95 10.24% 5000 29 J 15 58 , , , 37| I I ‘ ' I , I ' ' ' 'I' T-I— r-T-y-i-T-T-T-j—TT-T—r-j-r-i—r-r-j-T-T—I—I—[— m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

5518.D GCMS0403.M Thu Apr 04 13:55:54.2002 Page 2

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