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GCMS unknown compound analysis, sample AE05518, April 2002

Machine-extracted title · confidence 100%

Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 10, 2002.

NYC-WTC_000059296–000059306

Folder label: “GCMS X 3/11/02 A 4/1/02

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Scanned page image, NYC-WTC_000059305
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NYC 9/11 Public Portal Document

Library Search Compound Report t C:\HPCHEM\1\DATA\APRO1O2\5518.D Vial: 9 Data File Acq On 1 Apr 2002 8:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Ethanol, 2,2,2-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

8.28 0.43 ug/1 63834 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2,2,2-trichloro- 148 C2H3C13O 000115-20-8 12 2 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 9 3 1-Tetnacosanol 354 C24H50O 000506-51-4 9 4 1-Hexacosanol 382 C26H54O 000506-52-5 9

i Abundance / Scan 352 (8.280 min): 5518.D (-) m/z 43.05 ld0.'00% 43 - 5000

R1 83 gg 125 8.00 8.20 8.40 8.60 ' I''' 11' m/z 124.85 15.64% m/2-> 20 40 60 80 100 120 140 160 180 200 220240 260 280 300 320 340 Abundance #6653 r EthanoU^, 2-tnchloro-......... .......................... . 1

5000 77 8.00 8.20 8.40 8.60 113 m/z 82.8,5 12.01% I I lil_ III, 150 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #12247; 2-ProparionQ. 1,1,1-tnchloro- 43

8.00 8.20 8.40 8.60 5000 m/z 81.85 10.63% 15 85 125 I'''' I n/z -> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #49775; 1-Tetracosanol " ..... . 43 8.00 8.20 8.40 8.60 m/z 96.85 10.43% 5000 83

rn/z-> 11 111

20 40 60 80 100 120 140 160 180 200 220 240 260 280300320 340 308 336 111111111111 8.00 8.20 8.40 8.60

5518.D .GCMS0403.M Thu Apr 04 13:55:59 2002 Page 3

NYC-WTC_000059305

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NYC-WTC_000059305Source: NYC Law Department, mirrored locally

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