GCMS analysis results for sample AE12573, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\JUN0302\12573.D Vial: 24 Acq On 4 Jun 2002 7:55 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 8.06 0.81 ug/l 55426 1,4-Dichlorobenzene-d4 12.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 -Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 83 2 5 - Hexen-2 - one 98 C6H10O 000109-49-9 9 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 5 4 2-Propanone, l-cycloprdpyl-_____ 98 C6H10O 004160-75-2 4 Abundance - Scan 329 (8.062 min): 12573.D (-) m/z 43.00 100.00% 43

5000 59

101 —Pnm—TTTTTTr 83 7.80 8.00 8.20 8.40 t | 51 1l m/z 59.00 48.52% ■ ‘ i ■ ■ ' 1 i • 1 ■ ■ । ■ ■ • t 1 ■ ‘ * i * 1’1 r / 14 mlz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ■ • i 1 ■ ■ 1 i ' ■ ■ * i ■ • 1 ■ i • ■ 59 7.80I 8.00 8.20 8.40 m/ z i58.00 20.38% 15 31 . | I 83 _ 101 ] 11 i ■ ■ • ■ i ■ 1 ■ ■ i‘ ■ TTT 1 1* 11 ————— miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one 43 __ 7.80 8.00 8.20 8.40 5000 m/z 101.05 17.78% 55 15 27 50 . | 11/438 ' ' ' i 83 98 ' IIIBFEnUI Fr-rit । i 11 mz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- ■■ ।। . ■ ■

43 7.80 8.00 8.20 8.40 m/z 41.00 8.10%

5000 15 101 27 71

m/z—> ‘ ' I''1 10 56 ■ rr ■ 1,4 ■ ' ■ r TTPPPmm 20 30 40 50 60 70 80 90 100 110 MAA —AAA+ 7.80 8.00 8.20 8.40

12573.D GCMS0531.M Tue Jun 04 11:53:14 2002 Page 1

NYC-WTC_000014717