GCMS analysis results for sample AE12573, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JUNO302\12573.D Vial: 24 Acq On 4 Jun 2002 7:55 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.11 1.15 ug/1 77925 1,4-Dichlorobenzene-d4 12.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 39 2 N-Acetylpyrrolidone 127 C6H9N02 000932-17-2 9 3 2-Acetylthiazole 127 C5H5NOS 024295-03-2 5 4 2-Acetyl-1,4,5r6-tetrahydropyridine 125 C7H11NO 000000-00-0 5 Abundance Scan 334 (8.108 min): 12573.D (-) m/z 43.00 100.00% 43

5000

~rT I 1 1 T-n 49 61 83 97 117 125 7.80 8.00 8.20 8.40 37 >■! । I1! 1---------- m/z 124.95 10.74% niz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 4)3

5000 —.... .......... 7.80 8.00 8.20 8.40 m/z 96.90 7.36% 15 35 ,49 85 97 117 125 — m/z-> 10 20 30 40 50 60 70 80 90. 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone 43 1 ■ i ■ ■ ■ ‘ i ■ 1 ■ ■ i 1 1 1 1 I ' 1 1 ' I

7.80 8.00 8.20 8.40 5000 m/z 82.85 6.79% A 99 127

1956 o 30 86 112 ’ 1***1* — 144-11144*1-441111 V miz-s 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4717:2-Acetylthiazole ■ 1 ■ i ‘ 1 1 1 i 1 1 rl ’ 1***’I 43 7.80 8.00 8.20 8.40 m/z 98.90 6.36% 5000 99 127 58 112 85 33 '| ' ' । ' l 1 'T' I । । । ' I 1 ' ' ' I ' 1 ' ' I __________ H____________ ■ ■ i ■ ■ ■ • i ■ ' ■ ■ i1 • ■' i ■ ‘ • ■ i ' ■ 1 1 I 1 1 1 ''i 1 ' 1 ' ' i ■ ■ ' • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ I miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40

12573.D GCMS0531.M Tue Jun 04 11:53:15 2002 Page 2

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