GC/MS analysis results, sample AE10605, May 10 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY1002\10605.D Vial: 7 Acq On : 10 May 2002 6:55 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-amino-4-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 8.68 2.06 ug/1 163339 1,4-Dichlorobenzene-d4 12.17 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Penta: ne, 4-amino-4-methyl- 115 C6H13NO 000625-04-7 40 2 Propana 58 C3H60 000123-38-6 9 3 2-Propanamine, 2-methyl- 73 C4H11N 000075-64-9 9 4 Trimethylene oxide 58 C3H60 000503-30-0 7 Abundance Scan 397 (8.675 min): 10605.D (-) m/z 58.10 ioo.oo%| 58

5000 43

100 8,40 8.60 8.80 9.00 ....................... 38, 51 , i TTTTTTTTTTTTT TTTTpTTrpTTTpnnTpnTnYTTTT^^ 83 TCmnTg—mgumn 91 | m/z 43.05 34.31% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #3147:2-Pentanone, 4-amino-4-methyl- 58

5000 —■ ■ ' ■ | 1 I ' 1 | I ' ' ' |V' . . I . . . I 8.40 8.60 8.80 9.00 42 m/z 42.05 20.59% 100 30 35 1 49 TTPTT*TTTTTTTTTTTT+ + I " ‘' I" " I 84 “ 'i'"■ r1 ■ 'i | " r " ■ i" ''I m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #62332: Propanal 23 58

8.40 8.60 8.80 9.00 5000 m/z 100.10 11.46%

miz—> H11111"' I" " I ll' +9..... 53, 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #62536: 2-Propanamine, 2-methyl- ■ • i ■ ■ 58 8.40 8.60 8.80 9.00 m/z 41.05 8.72% 5000

15 41

m/z-> " " i" " ‘ ‘IT 130.. . .. 1 ■!11''i11 —pgTT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ' ' i 0) ''’i'1 ' ' ' i ' 1 ' ' T' 13? 8.40 8.60 8.80 9.00

10605.D GCMS0510.M Mon May 13 09:31:52 2002 Page 2

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