GCMS method and data sheet, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\LBB.D Vial: 13 Acq On : 10 Dec 2001 10:26 pm Operator: 209 GALOS Sample :. gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 n-Hexylmethylamine Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

37.17 0.62 ug/1 87078 Perylene-dl2 37.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual l n-Hexylmethylamine 115 C7H17N 035161-70-7 3 2 Nitrous ide 44 N20 010024-97-2 3 3 2-Propanol, 1-amino- 75 C3H9NO 000078-96-6 3 4 Carbo® dioxide 44 CO2 000124-38-9 3 Abundance Scan 3499 (37.168 min): LBB.D (-) m/z 39.95 100.00% i . 40

5000

' i ■ • • • i ' ■ TT—mrraf 36.80 37.00 37 20 37.40 66 97 115 177 209 281 TIp—nitt T, । TT TT110011100*0unTmT—T_TE1111111O21 TIr m/z 43.95 60.43% miz-s 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #3165: n-Hexylmethylamine 41

5000 TTTTTTA T PTr Trr Fr 36.80 37.00 37.20 37.40 m/z 115 .10 1.81% 27 . 57 70 115 PT I | If! I TT miz-> 20 40 160 80 100 120 140 160 180 200 220 240 260 280 Abundance

5000 30 44

| #39: Nitrous Oxide

m/z TIPr JU 36.80 37.00 37.20 37.40 35.90 TI4pr

1.52% 14 | |

TTUOmamamppmmnTr J l miz-? 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #353:2-Propanol, 1 -amino- ’ ' * ...... l 30 36.80 37.00 37.20 37.40 m/z 50.00 0.88% 5000 44 58 15

- 72 ‘11 ■ 11' 1' i ‘ ■111 ‘ ‘ ' I i • ‘ ■ i ■111 i'11 * i11 ‘1111 ' ■ i • ■ • • i'1 l i il...... $ 118S 1[ TT 1 I ' LB m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 36.80 37.00 37.20 37.40

LBB.D GCMS1126.M Wed Dec 19 13:11:11 2001 Page 4

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