GCMS method and data sheet, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\LBB.D Vial: 13 Acq On : 10 Dec 2001 10:26 pm Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.42 1.75 ug/1 378557 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tent at ive]ID MW MolForm CAS# Qual 1 2-Propanol, 1- -methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3/3 ‘-oxybis- 162 C8H18O3 054305-61-2 50 3 1 - Propanol, 2 - (2 - hydroxypropoxy) - 134 C6H14O3 000106-62-7 45 4 2-Propa: Abundance 7 -[(1-methyl-1,2-eth 1,1,1 Scan 694 (11.417 mln): LBB.D (-) 192 C9H2004 001638-16-0 42 m/z 59.05 100.00% 59

5000 45 103 73 i • ‘ 1 ■ i ■ 1 TIr 39. 11.00 11.20 11.40 11.60 11.80 89 । 130 — I— — 1 - TTLICEC—uussT—r 111111/7 TI—anugr m/z 44.9.5 45.27%

N. m/z~> 20 30 40) 50 60 70 80 90 100 110 120 130 140 Abundance ’ #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59

5000 103 T T T T T 45 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.05 34.77%

5000 • i * • • * UTT >‘|i 20 Abundance.... 30

31 40 T TTT r —It ‘I —er

45 50 60 70 80 90 — TI 'r-p-T-r-rT-r-r-r-r-i-ri-r-r-p- 100 #12859: 2-Butanol, 3,3‘-oxybis- 59

103 110 120 130 130 140

1 — -PP ’ I ‘ ‘ ‘ 4 I ’ * 'TT r 11.00 11.20 11.40 11.60 11.80 m/z 73.00 L 27.02%

TPT-P- 134 . TInunupunif m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 11.00 11.20 1140 11.60 11.80 m/z 41.05 23.19% 5000 31 45 103

75 . 89 TI'Trturr TTm4 —T miz-> 20 30 40 50 160 70 80 90 100 110 120 130 140 11.00 11.20 1140 11.60 ’11.80

LBB.D GCMS1126.M Wed Dec 19 13:11:07 2001 Page 3

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