GCMS blank results for sample AD29024, Dec 18 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\LBC.D Vial: 25 Acq On : 11 Dec 2001 12:05 pm Operator: 209 GALOS Sample : gc/ms scan 11/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 11.42 0.62 ug/1 186276 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, l-(2 ethoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,1 -oxybis- 134 C6H14O3 000110-98-5 56 3 1-Propanol, 2/ (2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 4 2 - Propanol, 1-(2 -methoxypropoxy) - 148 C7H1603 013429-07-7 50 Abundance Scan 695 (11.424 mln): LBC.D (-) m/z 59.05 100.00% i 59

5000 45 73 103 111111888 , j , , , , p । । i । i । 39 . 11.00 11.20 11.40 11.60 11.80 44—5051 —460....70+ 80 84

N TTT -r-p-T-T-r-rr m/z 45.05 49.28% miz-2 30 40I 90 100 110 120 130 (Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy) 59

5000 l • • • • I —P—mmme 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.00 30.05% - 1 I'11' i1 — TT18s > p i i 130 i । r-r m/z-> 30 40 50 160 70 80 90 100 110 120 130 Abundance #8087; 2-Propanol, 1.1-xybis- 59 TTTTTTT 31 11.00 11.20 11.40 11.60 11.80 5000 45 m/z 73.00 5.70% 103 89 72 1 ■ i1 ■1111 * —————— । I TT TI : i 1 TI—tr T[B 3.8 BIT 1 1 * I T 1 miz-> 30 40 50 6070 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- l ■ T1 1 1 I 1 1 1 1 1 1 1 59 11.00 11.20 11.40 11.60 11.80

N m/z 41.05 24.61% 5000 31 45 103

11 75 89 • * i* ' * ’I r — r —H4Ht ‘11/17071111111511 1101 231 pr-n-r-p-r m/z-> 30 40 50 (60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60 11.80

LBC.D GCMS.1126.M Fri Dec 21 15:04:53 2001 Page 3

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