GCMS method and data sheet, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC10 01\LBB.D Vial: 13 Acq On : 10 Dec 2001 10:26 pm Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.33 1.37 ug/1 297039 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy- 1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3 ’ -oxybis- 162 C8H18O3 054305-61-2 64 3 1-Propa: , 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 59

T 4 2-Propanol, 1,1'-oxybis-___________ 134 C6H14O3 000110-98-5 50 Abundance Scan 685 (11.335 mln): LBB.D (-) m/z 59.05 100.00% i 59

5000 45 73 103

39. 11.00 11.20 11.40 11.60 — i : 1 1 11 lUi 51 — —.. 4 85 ■ i • ■ • • i ■ ।...................... 130........... m/z 45.05 miz-? 20 30 40I 50 60 70 80 90 100 110 120 130 140 Abundance.......... #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy) 1 59

5000 103 11 T T T T 45 11.00 11.20 11.40 11.60 73 31

— I ■ " »11 - .................. 130......... mz-s 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3°oxybis- 59

11.00 11.20 11.40 11.60 m/z 73.00 29.55%

NA 5000 31 45 103

I ................... ......... ........... . .................. ■................ 134 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 •Abundance ! #6086: 1-Propanol,2-(2-hydroxypropoxy)- 59 11.00 11.20 1140 11.60 ‘1 m/z 41.05 26.55%

I miz-> 5000 31 45

TITIIT > > । I । r > । । । r 20 30 40 50 I60 75 89 103

* I • • * • ! 1 ‘ ‘ * I ' * ‘ ‘ i • 70 80 90 100 110 120 130 140 _ AA 11.00 11.20 11.40 11.60

LBB.D GCMS1126.M Wed Dec 19 13:11:02 2001 Page 2

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