GCMS blank results for VOCs, sample AE12535, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\JUNO302\LBA.D Vial: 13 Acq On 3 Jun 2002 9:01 pm Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Propoxyamphetamine Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 37.73 0.87 ug/1 36715 Perylene-dl2 37.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Propoxyamphetamine 193 C12H19NO 000000-00-0 3 2 2-Hexanamine, 4-methyl- 115 C7H17N 000105-41-9 3 3 Tuaminoheptane 115 C7H17N 000123-82-0 3 4 1-Octanamine 129 C8H19N 000111-86-4 3 Abundance V Scan 3560 (37.726 min): LBA.D (-) m/ z 39.90 100.00% 47

5000

Pm PT rrn TTEman 132 37.40 37.60 37.80 38.00 116 193 207 232 253 TImWBBI—BBTRBmTT ■ i ■ ‘ ■ i 1 ■ ■ ■ i ' ■ ' ■ i ■ ■ ■ 1 i ■ ‘ ■ i ■ ■ ■ ■ i m/z 43.90 63.91% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #21000:3-Propoxyamphetamine 44

5000 ■' । ■' ■ * । • ■ ■ ■ ।1 ■ ■ ■ । ■ ■ ■ ■ । 37.40 37.60 37.80 38.00 77 107 m/z 131.70 9.27% ■ I ■ i ' " '"I ' .. 133 150 . . 178 ........ . ... । । । T mlz-> 20 40 60 80 IPO 120 140 160 ■ 180 200 220 240 Abundance #64246:2-Hexanamine, 4-methyl- 41

37.40 37.60 37.80 38.00’’ 5000 m/z 129.30 5.02%

27 5583190 115 lii i

miz-> 20 60 80 100 120 140 160 180 200 220 240’ i ' ■ • ■ I 40 Abundance #64244: Tuaminoheptane 44 * 1 i • » • > i - ’I 37.40 37.60 37.80 38.00 m/z 207.00 3.09% 5000 AIwMWwWWw

30 i1 "i *!" 55 78 ‘ ' i ‘ ‘ ‘ ‘ i ‘ 100 AK ________________________ ‘ ‘ I ‘ ‘ i ‘ ‘ ‘ ‘ i 1 ■ ' ■ i ■ ■ ' ■ I • ■ ■ ■ i ‘ ■ ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 37.40 37.60 37.80 38.00

LBA.D GCMS0531.M Tue Jun 04 11:53:39 2002 Page 2

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