Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
NYC-WTC_000033886–000033901Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV2601\LBA.D Vial: 9 Acq On : 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample : 11/20 lab bik scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Monolinoleoylglycerol trimet Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
36.72 0.91 ug/1 176851 Perylene-dl2 37.12
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 23 2 l,l,l,5,7,7,7/Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 17 3 Tris(trimet 1silyl)borate 278 C9H27BO3Si3 004325-85-3 12 4 1,2-Benzene icarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 10 Abundance ( Scan 3451 (36.723 min): LBA.D (-) m/ z 73.00 100.00% 73
147 5000 221 281 355 TIT __ J _
miz-> 43 50 , 94 119, . THT T 1 ' 1 1 ’ 1 ' — 100 150 191 14 200 250 ( TT 300 29 1 325. i 350. .. 429 401 I--PIi 400 450 — 36.40 36.60 36.80 37.00 ____ m/z 147.00 65.56% Abundance #58871:1-Monolinoieoylglycerol trimethylsilyl ether 73
207 5000 147 °—TTfTmo I I [. —PT 36.40 36.60 36.80 37.00 34 I 103 m/z 221.05 48.88% II 1 281 — ------------------ | 395 482 11 I m/z-> 50 100 150 200 250 300 350 400 450 Abundance #56714:1.i.1.5.7.7.7-Heptamethyl-3.3-Ws(trimethylsWoj<v)t 73
147 36.40 36.60 36.80 37.00 5000 267 m/z 281.00 28.32% 355 429 45 207
I 100 ' ' 150 ‘ ' 200 250 ‘ 300 ' 350 ' ' 400 ' 450 m/z-> 50 Abundance #39028: T ris(trimethylsilyl)borate 73 221 36.40 36.60 36.80 37.00
X_ m/z 354.9, 5000 263 133 175 ■ 1 i ’ ■ miz-> 50' ' ' 100 ' ' 150 ' ' 200 ' 250 300 350 400 450 36.40 36.60 36.80 37.00
LBA.D GCMS1126.M Thu Jan 03 12:52:15 2002 Page 3
NYC-WTC_000033894
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NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
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Header page for a gas chromatography-mass spectrometry scan file related to environmental testing at the World Trade Center site.
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Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047955
GCMS blank analysis report for sample AE08209 listing volatile organic compounds from April 2002.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder