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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086788–000086807

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086804
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample 9/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Tetratetracontane Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

35.53 0.40 ug/1 63268 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolFonn CAS# Qual

1 Tetratetracontane 619 C44H90 007098-22-8 91 2 Hexatriacontane 507 C36H74 000630-06-8 91 7 3 Tritetracontane 605 C43H88 007098-21-7 91 / 4 Octadecane 254 C18H38 000593-45-3 90 / Abundance Scan 3321 (35.527 min); LBC.D (-) m/z 57700 100.00%

85 5000

T 35.20 35.40 35.60 35.80 207 282 m/z 71.10 70.79% Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74745: Tetratetracontane 57

253 85 35.20 35.40 35.60 35.80 m/z 77705 667744% ................................................... I , 463491519M7 ■ 591618 ' ' ' I ' 160 150 2t^ 250 300 350 400 450 500 550 600 Tlfe->52 Abundance #74635: Hexatriacontane 57 7 35.20 35.40 35.60 35.80 5000- 85 m/z 85.05 50.35%

! j.fy. 1 . , , , I , . . . I, , , . I. . . , I....... n/z->____ 52 100 150 200 250 300 350 400 450 500 550 600 Abundance #60913; Tritetracontane 57 35'20 35.4'0 '35'60' '35'80 ' m7z 55700 23.12% 5000 85

1 ........................................................................................................... ioo 150 '200 250 ' 360 350 400 450 500 550 600 ■n/z-> 50 35.20 35.40 35.60 35.80

LBC.D NP091101.M Tue Oct 02 12:17:45 2001 Page 11

NYC-WTC_000086804

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NYC-WTC_000086804Source: NYC Law Department, mirrored locally

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