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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086788–000086807

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086803
OCR text

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On 1 Oct 2001 3:40 pm Operator: 2 09 GTkLOS Sample 9/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Heneicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 33.72 0.53 ug/1 93842 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91-^ 2 Pentacosane 352 C25H52 000629-99-2 91 / 3 Tetracosane 338 C24H50 000646-31-1 91 / 4 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91/ flibundance Scan 3124 (33.718 min); LBC.D (-) m/z5770^ 100.00% 57 43 71

85 533

Ti/z-> 'Xbundance 40 w 60 80 100 120 140 160 180 200 220 240 260 280 300 320.340 #42201; Heneicosane 33.40 33.60 33.80 34.00 m/z 71.10 73.57%

57 71 85 5000 33.40 33.60 33.80 34.00 99 m/z 43.05 7076^% LI,,, )i, J',, . ........ ........... I,... I. . I....... n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73718: Pentacosane 43 57 TTTTTTTTTi 33.40 33.60 33.80 34.00 71 5000 m/z 85.05 50.00% 85

I ^^P1?7141155169183197211225 I i I T l Y 1^1 .Y t | T i I I j' n . r I I . I . k i . I . . I . I 1 . J , I 11' 111' " 1111" I ■nte-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5 7 33.40 33.60 33.80 34.00 71 m/z 41.00 26.12% 5sa 85

99 1 I' ' ' p4-TT^Y'rT-VTyrhTyrTTVpr1'TT-|-VT-TTY’'TTTyrTTT^^ 338 I''' 'I' T I ' ' ' ' I ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 33.40 33.60 33.80 34.00

LBC.D NP091101.M Tue Oct 02 12:17:41 2001 Page 10

NYC-WTC_000086803

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NYC-WTC_000086803Source: NYC Law Department, mirrored locally

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