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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086788–000086807

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086802
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On : 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample : 9/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Heneicosane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

32.76 0.40 ug/1 71903 Chrysene-dl2 33.16

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91^ 2 Octadecane 254 C18H38 000593-45-3 91 / 3 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 / 4 Tetracosane 338 C24H50 000646-31-1 91/ Abundance Scan 3020 (32.763 min): LBC.D (-) m/z 57.00 100.00% 57 71 43 5000 85

2k n/z-> <\bundance ukite 40 60 80 141155 183 207 281 Tpn-Tnq-T-TT-Tqn-TT-ryT-T-rTq-r-rT-T-p-r-rTyT-rT-ryT^^ 100 120 140 160 180 200 220 240 260 280 300 320 #42201: Heneicosane 32,40 32,60 32,80 33,00 m/z 71.00 79.05%

5)7 71 85 I . I I I I . I , /1 , I-.,- .-1-^_ 5000 32.40 32.60 32,80 33,00 99 m/z 43.00 63.68% 268 296 .1 I''' ‘ I'''' I' ''' I I ''' ' I ''' ' I' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71561: Ocladecane 5^ 43 71 32.40 32.60 32,80 33,00 85 m/z 47.97% 5000 85.05 ii

99 J .......... •nfe-> *\bundance 40 60

43 57 80 100 120 140 160 180 200 220 240 260 280 300 320 #50999: Eicosane, 7-hexyl- ... ,,..M.... 32,40 32,60 32,80 33,00 m/z 41.05 22.50% 71 5000 85

I I, ll 169'>82i97 310 281 J p-T^TTyHhnn^YTT^Tp-YTTYTT-TT-p'T'TT^^ I ‘' I '' I ' ' ' ' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 32,40 32,60 32,80 33,00

LBC.D NP091101.M Tue Oct 02 12:17:37 2001 Page 9

NYC-WTC_000086802

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NYC-WTC_000086802Source: NYC Law Department, mirrored locally

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