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GC/MS calibration table for TCLP analytes, October 2001

Machine-extracted title · confidence 90%

Calibration data table for TCLP analysis including retention times and response factors for various compounds.

NYC-WTC_000086981–000087006

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000086999
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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On : 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample : 9/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heneicosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 32.77 2.83 ug/1 440499 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91 2 Eicosane 282 C20H42 000112-95-8 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Octadecane 254 C18H38 000593-45-3 90 Abundance Scan 3020 (32.766 min): LBD.D (-) m/z 57.00 100.00% 57

85 4' 32.40 32^0 32.80 33.00 169 197 225 253 281 352 m/z ' I ' " I " ' '■ I " " I " ‘ ' I " " I " " I " " I " " I " " ( " 71.05 71.74% ■nfe-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #42201: Heneicosane ft 5)7

85 5000 32.40 32.60 32.80 33.00 m/z 47705 65774%

tVz-> 40 60 u 113 I''''I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 268 296 I' " ' I " '' I' p-TTTp-rrr-f

Abundance #39862: Eicosane 7

_3Z40_3260_J280_^3;00_^_ 5000 85 m/z 85.05 49771%

240 282 I ' ' ‘ ' I I ' ' 'I I I r. I I I I 1 I I I I I j 1 . I I I I I I I I I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71193: Heptadecane 57 3240 32.60 32.80 33.00 m/z 41.05 75795% 5000 85

J , 141 210 240 169 I''''I ' I " '' I'' " f' " ' I " '' I I' " ' I1111 I ‘" I' " • I " '' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

LBD.D NP091101.M Tue Oct 02 12:28:54 2001 Page 13

NYC-WTC_0(i(id86999

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NYC-WTC_000086999Source: NYC Law Department, mirrored locally

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