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GC/MS calibration table for TCLP analytes, October 2001

Machine-extracted title · confidence 90%

Calibration data table for TCLP analysis including retention times and response factors for various compounds.

NYC-WTC_000086981–000087006

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000087000
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On 1 Oct 2001 4:39 pm Operator:. 2 09 GALOS Sample 9/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* . Peak Number 14 Heneicosane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T, 33.72 3.38 ug/1 526321 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Octadecane 254 C18H38 000593-45-3 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Nonacosane 408 C29H60 000630-03-5 91 Abundance Scan 3124 (33.721 min): LBD.D (-) m/z SYTOO 100.00% 7

85 5000

nUlhuU T I 113 141 169 197 33.40 33.60 33.80 34.00 225 253 280295 366 ' I " " I' " ' I "'' I " " I " " I " " I " " I " " I' m/z 71.00 71708% TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 <\bundance #42201: Heneicosane 57

85 5000 33.40 33.60 33.80 34.00 m/z 43705 64.25% I 113 ■nfe-> 40 '' I' jUJXciu I I I 1 I|r.IqI.TiI ....(I I I I I 268 296 I''''I''*'1''''1 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 I'''' I''' 11' I ‘ ’ ’ ’ 1 ' ' ' ‘ I

Abundance #71561: Octadecane 5|7

33.40 33.60 33.80 34.00 85 5000 m/z 8570551752% J I 113 224 254 n/z-> Abundance I' '''I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 7 #71193: Heptadecane ..... R,.... 33.40 33.60 33.80 34.00 m/z 41705 23.97%

5000 85

" I" . . .R I"'' r ' ' ' I ' ' " ' I ' ' ’ ' I' ‘ .‘ .' .1^^ 210 240 I ' ''' I ' ' ' ' I ' ' ' 'I ' ' ' ' I■' ' 'I ‘ ___________ 'I '' ' ' I ' ' ' ' r ' ' ' I ' ' ' ' I ' ' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260280 300 320 340 360 33.40 33.60 33.80 34.00

LBD.D NP091101.M Tue Oct 02 12:28:58 2001 Page 14

NYC-WTC_000087000

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NYC-WTC_000087000Source: NYC Law Department, mirrored locally

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