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GC/MS calibration table for TCLP analytes, October 2001

Machine-extracted title · confidence 90%

Calibration data table for TCLP analysis including retention times and response factors for various compounds.

NYC-WTC_000086981–000087006

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000087001
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On : 1 Oct 2001 4:39 pm Operator: 209 GALOS Sample : 9/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params*. LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101 .M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ************************************************************************ Peak Number 15 Heneicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.64 2.62 ug/1 408698 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 3 Tetracosane 338 C24H50 000646-31-1 90 4 Octadecane 254 C18H38 000593-45-3 90 Abundance Scan 3224 (34.639 min): LBD.D (-) m/z 57.00 100.00% 71 43 553 85 .......... I I 34.40 34.60 34.80 35.00 . ,f| .'ft, ,4, 281295 m/z 71.05 70.18% I''''I'' '' I tt/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71

5000 85 L .... ''' I'' ‘' I'' 34.40 34.60 34.80 35.00 99 m/z 43.05 63.66% il j Tfiyiy 268 296 r ''' I''' * 1' I''''I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #50999: Eicosane, 7-hexyl- 43 57

71 IL 34.40 34.60 34.80 35.00 5000- 85 m^ 85.05 45.70%

1 li ''82197 281 310

It I* I r. I q-. . . . I . . . . , . . . .-| I' ' I ’''' I''' ' I ' I'''' I'''' I r ■n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane T 43 57 __3440_J£60_J48g_^5;00 71 m/z 41.05 23.38% 5000 85

88 in

Tl/Z-> 40 JU4 || ,1 '27 155169183197 I ' ' ' ' I ' ' ' ' I ' I' ' I I 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 294 338 I ' ' ' 'I ' ' ' ' I ' ' ' ' I I ' ' ' I I I ' ' I I ' ' ' I ' I I ' I ' 7 T 34.40 34.60 34.80 35.00

LBD.D NP091101.M Tue Oct 02 12:29:02 2001 Page 15

NYC-WTC_000087001

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NYC-WTC_000087001Source: NYC Law Department, mirrored locally

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