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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan”

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Scanned page image, NYC-WTC_000086782
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0101\LBA.D Vial: 2 Acq On 1 Oct 2001 2:41 pm Operator: 209 GALO Sample 9/14 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Heneicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.64 0.93 ug/1 211162 Chrysene-dl2 33.17 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91 2 Octadecane 254 C18H38 000593-45-3 90 3 Tetracosane 338 C24H50 000646-31-1 90 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 90 Abundance Scan 3225 (34.644 min): LBA.D (-) m/z 57.00 100.00% 5/ 43 71 85 5000

A 34,40 34,60 34,80 35,00 Wz 71.0.0 71.31% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71 85 k. 5000- 34.40 34.60 34.80 35,00 99 m/z 43.00 66.44%

iVz-> Abundance

5000- 40 p l I r| I n I j "r. Q . IT11 II I11111 I p

43 60 57 71 268 296 T I " • • r " 111 80 100 120 140 160 180 200 220 240 260 280 300 320 340

85 #71561: Octadecane □l m/z 34.40 34.60 34.80 35,00 85.0.5 52.13%

99 ma. 80 100 120 140 160 180 200 220 240 260 280 300 320 340 224 254 Ti/z-> 40 60 Abundance #73543: Tetracosane Tf I ■ ■ ■ ri ■ 'T' 1 ' 43 57 __3440_3£60_J48g_35W_ 71 m/z 41.00 24.19%

5000 85

99 , I I |1 \| 127 155169183197 338 294 p 11 11TI.. I.,. 11., I ■ 11 I .■'i I I r, 11, b1, I "" I' " N ' 'I' ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.40 34.60 34.80 35.00

LBA.D NP091101.M Tue Oct 02 12:02:53 2001 Page 9

NYC-WTC_000086782

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NYC-WTC_000086782Source: NYC Law Department, mirrored locally

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