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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan

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Scanned page image, NYC-WTC_000086783
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0101\LBA.D Vial: 2 Acq On : 1 Oct 2001 2:41 pm Operator: 209 GALO£ Sample : 9/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexatriacontane Concentration Rank 7

R.T. EstConc Area Relative to. I STD R.T. 35.53 0.88 ug/1 178927 Perylene-dl2 37.29 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Tetratriacontane 479 C34H70 014167-59-0 91 3 Heneicosane 296 C21H44 000629-94-7 90 4 Heptadecane 240 C17H36 000629-78-7 87 Njundance 1Scan 3322 (35.535 min): LBA.D (-) m/z 57700 100.00% 57

5000 85

' ' I ' ' ' ' I 35.20 35.40 35.60 35.80 m/z 71.00 64.08% nfe-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 3^^0 400' i\bundance #74636: Hexatriacontane 57

5000 85 35.20 35.40 35.60 35.80 m/z 43.05 61.41% I 11 , 141 . 169 197 p n. I fl. 11 NII I n 11 (i I 111. ij n. > I ■ ■ 111 I'"' I'"' I nfe-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #58265; Tetratriacontane 57

5^.20 35.40 35.60 35.80 5000- 85 m/z 85.00 48.82%

311 367 410 TiZz-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #42201; Heneicosane 57 35.20 35.40 35.60 35.80 m/z 41705 23.46% 85 5000

"'I" TlpHnTyTTTTYrT^rTprTT-pnTVpTT-TyTTTTyrrTTp-rnyrTTrrpn-rrj-rTTtpmTyrT^^ ■nA’-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 35,20 35,40 35.60 35.80

LBA.D NP091101.M Tue Oct 02 12:02:55 2001 Page 10

NYC-WTC_000086783

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NYC-WTC_000086783Source: NYC Law Department, mirrored locally

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